http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109622044-B

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filingDate 2018-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-07-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-07-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109622044-B
titleOfInvention Efficient hydrogen evolution catalyst material, preparation method and application
abstract The invention relates to a preparation method of a high-efficiency hydrogen evolution catalyst material, which comprises the following steps: 1) preparation of palladium ammonium complex: adding palladium chloride and ethylenediamine into deionized water for ultrasonic treatment; 2) dispersing ammonium tetrathiomolybdate and urea in N, N-dimethylformamide to form a homogeneous solution; transferring the palladium-ammonium complex into the solution, carrying out ultrasonic treatment, adding hydrazine hydrate, and continuing ultrasonic treatment; 3) adding the obtained solution into a reaction kettle and reacting for 4 hours at the temperature of 160-; 4) and after the reaction is finished, naturally cooling to room temperature, carrying out solid-liquid separation, washing and drying the precipitate, and calcining the obtained sample at 400 ℃ for 2h in a hydrogen environment to obtain the material. The high-efficiency hydrogen evolution catalyst material can obviously improve the Hydrogen Evolution (HER) performance of the catalyst.
priorityDate 2018-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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