http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109557232-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N2030-8813 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-88 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-88 |
filingDate | 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-109557232-B |
titleOfInvention | A kind of detection method of arsanilic acid, nifediarsenic acid and roxarsine in eggs |
abstract | The invention relates to a method for the determination of arsanilic acid, nifediarsenic acid and roxarsone in eggs by liquid chromatography tandem mass spectrometry, and belongs to the field of residue detection. Add 1% formic acid water-acetonitrile (30:70, V/V) to the extraction solution to the sample to be tested, vortex and mix, centrifuge, repeat the extraction twice, combine the supernatant, defatted with n-hexane, and concentrated to less than 40°C by rotary evaporation. 3mL, dilute to 5mL with 10% methanol aqueous solution, centrifuge, filter the supernatant through membrane, and use high performance liquid chromatography-tandem mass spectrometer for determination. The invention has high accuracy, precision and sensitivity, and fills the blank of simultaneous detection of three kinds of organic arsine preparations in eggs. |
priorityDate | 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 46.