http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109557232-B

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-88
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-88
filingDate 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109557232-B
titleOfInvention A kind of detection method of arsanilic acid, nifediarsenic acid and roxarsine in eggs
abstract The invention relates to a method for the determination of arsanilic acid, nifediarsenic acid and roxarsone in eggs by liquid chromatography tandem mass spectrometry, and belongs to the field of residue detection. Add 1% formic acid water-acetonitrile (30:70, V/V) to the extraction solution to the sample to be tested, vortex and mix, centrifuge, repeat the extraction twice, combine the supernatant, defatted with n-hexane, and concentrated to less than 40°C by rotary evaporation. 3mL, dilute to 5mL with 10% methanol aqueous solution, centrifuge, filter the supernatant through membrane, and use high performance liquid chromatography-tandem mass spectrometer for determination. The invention has high accuracy, precision and sensitivity, and fills the blank of simultaneous detection of three kinds of organic arsine preparations in eggs.
priorityDate 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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