http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109553639-B

Outgoing Links

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-5004
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-505
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-50
filingDate 2018-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-10-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-10-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109553639-B
titleOfInvention Method for synthesizing tri-tert-butylphosphine
abstract The invention discloses a method for synthesizing tri-tert-butylphosphine, and belongs to the field of organic synthesis. In an anhydrous and oxygen-free atmosphere, bromo-tert-butane is used as a raw material and reacts with calcium phosphide under the catalytic action of a nickel catalyst to generate tri-tert-butylphosphine. Compared with the prior art, the method has the advantages of mild reaction conditions, simple operation, high yield, simple and easily obtained raw materials, reduction of production cost and suitability for industrial production.
priorityDate 2018-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 36.