http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109516908-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_87b3f9f9968c1dfd87f754a4e66a357f |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C45-78 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C49-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C45-78 |
filingDate | 2017-09-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_940452533be0709611748eaa6965a895 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2ff6c3152b9c5e603a139f7a2712051a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b82c232565a9a951648fc069cfb0d429 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f526bb1932abad71794f27bb3f3dbfe0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e03c4fdf7e3e97d5684be1f011851175 |
publicationDate | 2019-03-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-109516908-A |
titleOfInvention | Purification method and application of 1,1,3-trichloroacetone |
abstract | The invention belongs to the technical field of compound purification, and specifically relates to a purification method of 1,1,3-trichloroacetone and its application, wherein the method comprises the following steps: (1) combining 1,1,3-trichloroacetone crude product with (2) recrystallize the upper layer solution after standing; and (3) filter out and wash the recrystallized solid crystals; wherein, the 1,1,3-trichloro The weight ratio of the consumption of acetone crude product and water is 1: (0.1-2). The method is environmentally friendly, and greatly reduces the generation of waste water, and does not produce waste organic solvents and organic waste gases; in addition, the aqueous solution of 1,1,3-trichloroacetone purified by the purification method is directly used in the production of folic acid, Side reactions are reduced, the total yield of folic acid can be increased by 5% by weight, the purity is above 99.2% by weight, and high-quality folic acid can be obtained. |
priorityDate | 2017-09-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 32.