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filingDate 2017-09-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_940452533be0709611748eaa6965a895
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publicationDate 2019-03-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109516908-A
titleOfInvention Purification method and application of 1,1,3-trichloroacetone
abstract The invention belongs to the technical field of compound purification, and specifically relates to a purification method of 1,1,3-trichloroacetone and its application, wherein the method comprises the following steps: (1) combining 1,1,3-trichloroacetone crude product with (2) recrystallize the upper layer solution after standing; and (3) filter out and wash the recrystallized solid crystals; wherein, the 1,1,3-trichloro The weight ratio of the consumption of acetone crude product and water is 1: (0.1-2). The method is environmentally friendly, and greatly reduces the generation of waste water, and does not produce waste organic solvents and organic waste gases; in addition, the aqueous solution of 1,1,3-trichloroacetone purified by the purification method is directly used in the production of folic acid, Side reactions are reduced, the total yield of folic acid can be increased by 5% by weight, the purity is above 99.2% by weight, and high-quality folic acid can be obtained.
priorityDate 2017-09-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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