http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109499093-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_4a071870fce08ce23a3fcb4a4f790e46
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01D11-02
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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01D11-02
filingDate 2018-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ead5c0b3c8683b90132bf4c4942f5bca
publicationDate 2019-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109499093-A
titleOfInvention A kind of broken-wall extraction technology of amino acid in soybean
abstract The invention discloses a wall-breaking extraction process of amino acids in soybeans. The steps are as follows: 1) crushing fresh soybeans, using petroleum ether or solvent gasoline or a mixture of the two as a solvent to perform reflux extraction on the material twice, and during extraction, the solvent and The volume-to-mass ratio of the material is 3:2-18:2, and the extraction time is 8 hours. During the extraction process, the extraction tank is subjected to intermittent vacuuming and vacuum breaking, and the two extracts are combined and concentrated for later use; the concentrated soybean The liquid extract was subjected to silica gel column chromatography, followed by elution with a mixture of n-hexane and diethyl ether. The invention adopts the technology of combining multiple enzymes, effectively destroys the cell wall of the cells, increases the mass transfer area of the amino acid substances diffusing to the ethanol in the subsequent extraction process, and significantly improves the extraction rate of amino acids.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111111255-A
priorityDate 2018-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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