http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109337113-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08J9-286 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08J9-28 |
filingDate | 2018-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2021-07-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2021-07-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-109337113-B |
titleOfInvention | Monolithic material for embedding porous organic molecular cage and preparation method of monolithic column |
abstract | The invention provides a preparation method of an integral material for embedding a porous organic molecular cage, which comprises the following steps: dissolving a functional monomer containing two or more methacrylate groups in a pore-foaming agent, uniformly mixing, adding an organic molecular cage, uniformly mixing, adding an initiator, continuously uniformly mixing, placing in a sealed container, and carrying out free radical polymerization reaction on the monomer to form the integral material of the organic molecular cage with embedded pores in situ. Also provides a preparation method of the monolithic column, before the free radical polymerization reaction, the mixture is introduced into a capillary tube, sealed and started to carry out the free radical polymerization reaction; after the reaction is completed, the obtained monolith was washed with methanol or ethanol. The method has mild preparation conditions and simple method, the aperture and the pore structure of the whole material can be regulated and controlled by changing the content of the added functional monomer or the composition and the content of the pore-forming solvent, and the material is an organic material and has higher mechanical strength and larger specific surface area. |
priorityDate | 2018-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 36.