http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109313167-A

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filingDate 2017-04-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_be64787bfa8f8ea9a08356725d3532ac
publicationDate 2019-02-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109313167-A
titleOfInvention Polycapillary column preconcentration system for enhanced sensitivity in gas chromatography (GC) and gas chromatography-mass spectrometry (GCMS)
abstract A polycapillary column preconcentration trap (300) is disclosed for use in various chromatography techniques such as gas chromatography (GC) or gas chromatography-mass spectrometry (GCMS). The trap (300) includes a first trap (204) comprising a plurality of capillary columns (208A, 208B) connected in series in order of increasing intensity (ie increasing chemical affinity for one or more sample compounds) , 208C). The sample enters the trap (204), from the sample vial (202) into the relatively weak column (208A) of the trap to the relatively strongest column (208C), for example via any additional columns contained in the trap in between (208B). The trap is backwashed so that the sample flows out of the trap through the relatively weak head of the column. The trap can be further heated to aid in sample desorption. Next, the sample can be injected into a chemical analysis device (206) to perform chromatography techniques (eg, GC or GCMS), or the sample can be injected into a second trap (304) for further concentration.
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