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filingDate 2018-11-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-07-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-07-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109293464-B
titleOfInvention Method for effectively separating and purifying 2-methylnaphthalene from wash oil
abstract The invention discloses a method for effectively separating and purifying 2-methylnaphthalene from wash oil, which comprises the following steps: firstly, preparing a catalyst; and then preparing a target product by adopting a device consisting of a rectifying tower A, an isomerization reactor and a rectifying tower B, firstly placing the wash oil fraction in the rectifying tower A for reduced pressure distillation to prepare a methylnaphthalene enriched liquid, then placing the prepared methylnaphthalene enriched liquid in the isomerization reactor for reaction by adding a self-made catalyst, placing the filtered liquid in the rectifying tower B for reduced pressure distillation, and finally freezing, crystallizing and squeezing to prepare the target product. The method has the advantages of simple operation, low preparation cost, good storage stability of the prepared solvent, high boiling point and high yield.
priorityDate 2018-11-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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