http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109273731-A

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filingDate 2018-09-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b61cfe780c6e8f95a02494f794274bfb
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publicationDate 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109273731-A
titleOfInvention 3D porous network structure Pd3Pb alloy and preparation method thereof and application thereof
abstract The invention discloses a preparation method of a 3D porous network structure Pd 3 Pb alloy, which comprises the following steps: firstly, a surfactant Brij-58 is dissolved in a solvent of DMPU to prepare a solution having a concentration of 0.15-0.3 mol/l. Ultrasonic 2-10 min, then magnetic stirring for 20-40 min to form a uniform dispersion; followed by adding 1 -3 mL of octadecene to the dispersion and stirring for 2-10 min to form micelles; The palladium source and the lead source are first dispersed in 5-10 ml of distilled water in a molar ratio of 3:1, and ultrasonically formed for 2-10 min to form a uniform mixed solution; then the mixed solution is added to the micelle and stirred. 20-40 min, a uniform micelle solution is formed; finally, tetrabutylammonium borane is added to the micelle solution, and charged into the reaction vessel, and the temperature is raised and reacted for 8-12 hours. After being naturally cooled to room temperature, the mixture is centrifuged. Washing and drying to obtain a Pd 3 Pb alloy of a 3D porous network structure. The preparation method of the invention is simple, the performance is excellent, the stability is good, and the Pd 3 Pb alloy prepared according to the hydrothermal method exhibits excellent electrocatalytic ORR performance.
priorityDate 2018-09-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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