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publicationDate 2019-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109273280-A
titleOfInvention Flexible composite electrode material and preparation method and application thereof
abstract The invention belongs to the field of preparation of supercapacitor electrode materials, and in particular relates to a flexible composite electrode material and a preparation method and application thereof. The specific preparation method of the flexible composite electrode material of the invention is as follows: the graphene oxide, the H 2 SO 4 and the phytic acid are uniformly mixed in an aqueous solution, transferred to a hydrothermal kettle, and hydrothermally reacted to obtain a phosphorous-phosphorus doped graphene; The anhydrous antimony pentoxide is mixed with hydrofluoric acid, transferred to the reaction kettle, and hydrothermally reacted. To the obtained reaction liquid B, ammonium oxalate, sulfur-phosphorus-doped graphene and cobalt nitrate are added, and then the melamine sponge is placed. The temperature is increased, and the methylamine solution is added to obtain a cobalt ruthenium precursor; the melamine sponge is calcined under nitrogen to obtain a CoNb 2 O 6 /sulfur phosphorus-doped graphene/melamine sponge flexible composite electrode material. The reaction condition of the invention is mild, easy to control, and simple in process; the prepared CoNb 2 O 6 has good dispersibility and uniform size controllability, and is used as a supercapacitor flexible electrode with high reversible specific capacitance, and is expected to be industrially produced.
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type http://data.epo.org/linked-data/def/patent/Publication

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