http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109265687-B

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Predicate Object
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G77-398
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G77-398
filingDate 2018-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-04-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-04-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109265687-B
titleOfInvention Preparation method of polycarbosilane containing heterogeneous elements
abstract The invention discloses a preparation method of polycarbosilane containing heterogeneous elements. The method comprises the steps of taking liquid low-molecular-weight poly-silicon carbosilane and halide or organic complex containing heterogeneous elements as raw materials, placing the raw materials in a high-temperature high-pressure reaction device, vacuumizing and sealing the reaction device under the condition of an alkali metal silicon-aluminum compound catalyst, heating the reaction device to 350-450 ℃, carrying out closed reaction, cooling the reaction device to room temperature after the reaction is finished, and discharging gas in the reaction system to obtain a crude product containing the heterogeneous elements, namely the poly-silicon carbosilane. The method can shorten the reaction time and improve the preparation efficiency, and the prepared precursor has less branching and cyclic structure and higher Si-H content, thereby being beneficial to the improvement of the spinnability of the precursor and the control of the oxygen content and the structure in the ceramic process.
priorityDate 2018-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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