http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109233323-B

Outgoing Links

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09B23-16
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09B23-04
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D333-60
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D333-60
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B23-04
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B23-16
filingDate 2018-10-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-10-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-10-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109233323-B
titleOfInvention Preparation method of disperse blue 354
abstract A preparation method of disperse blue 354 is characterized by comprising the following steps: the method comprises a preparation step of a compound Ib, wherein in the step, methanol is used as a solvent, and a compound Ia and malononitrile are reacted in a mass ratio of 1:0.4-0.5 in the presence of piperidine, wherein the reaction temperature is 45 ℃ to the reflux temperature of the methanol. The step can reduce the dosage of malononitrile, has mild reaction conditions, reduces the generation of harmful substances, and has good product purity and high yield. The method has low cost of starting raw materials and high total yield.
priorityDate 2018-10-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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