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filingDate 2017-07-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109219611-B
titleOfInvention Crystal form of dapagliflozin intermediate and preparation method thereof
abstract A crystal form of an intermediate of Dapagliflozin and a preparation method thereof are disclosed, and the intermediate of Dapagliflozin (2S, 3R, 4S, 5S, 6R)-2-(4-chloro-3-(4) is specifically disclosed -Ethoxybenzyl)phenyl)-2-ethoxy-6-(methylhydroxy) tetrahydro-2H-pyran-3,4,5-triol crystal form and preparation method thereof. The advantages are that the intermediate can be highly purified to obtain a sample with a purity of more than 99.3%, which is of great significance for improving the quality of dapagliflozin, and the preparation process is simple and suitable for industrial production.
priorityDate 2016-07-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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