http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109134398-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_c55242fbf57a07c41db29a09b0a03530 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D277-593 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D277-593 |
filingDate | 2018-09-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c3d743098f036adc700cadc91ed15740 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ac118e4692b0a49aac80fcc47b209e78 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5aeb88dcf071cab877d499109bc1a18b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_83a384b0fbc5997ed50bca600a52dfcb http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_62c83ab8b65bb1571f0392fff70ea17d |
publicationDate | 2019-01-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-109134398-A |
titleOfInvention | The preparation method of high-purity ethyl demethylaminothiazolyloximate |
abstract | The invention belongs to medical synthesis technical fields, are specifically related to a kind of preparation method of high-purity ethyl demethylaminothiazolyloximate.Mixed solvent, insulated and stirred after heating are added into ethyl demethylaminothiazolyloximate crude product;Hydrochloric acid regulation system pH is added, after system dissolved clarification, active carbon is added and reducing agent is stirred;Be filtered to remove active carbon, filtrate with organic base regulation system pH in 4.5-6.5, then insulation reaction;Cooling rejection filter obtains ethyl demethylaminothiazolyloximate fine work.The preparation method of high-purity ethyl demethylaminothiazolyloximate of the present invention, simple process effectively raise the purity of ethyl demethylaminothiazolyloximate, and purity optimizes product quality 99.85% or more, at low cost, high income, are suitble to industrialized production. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114014823-A |
priorityDate | 2018-09-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 61.