http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109133168-A

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filingDate 2018-08-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9735f449313f67a2fefebe07dc599984
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publicationDate 2019-01-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109133168-A
titleOfInvention A kind of preparation method of monoclinic truncated octahedral bismuth vanadate crystal
abstract The invention relates to a preparation method of monoclinic phase truncated octahedral bismuth vanadate crystal, which comprises: obtaining solution A through bismuth nitrate pentahydrate, nitric acid solution and fluoride ion solution water; obtaining the solution through ammonium metavanadate and sodium hydroxide solution B; obtain solution C through the solution B and the solution A; perform a microwave hydrothermal reaction on the solution C to obtain a crystal sample; wash and dry the crystal sample to obtain the monoclinic phase truncated eight Hedral bismuth vanadate crystals. The invention adopts microwave hydrothermal reaction to prepare bismuth vanadate crystal, and by controlling parameters such as the molar ratio of fluoride ion to bismuth ion, reaction temperature, reaction time, etc., the bismuth vanadate crystal with monoclinic phase truncated octahedron is prepared and synthesized, and the prepared bismuth vanadate crystal is obtained. The crystals have the characteristics of high purity and good photocatalytic performance.
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priorityDate 2018-08-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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