abstract |
The present invention relates to a kind of graphene micro-flowers/nano zinc oxide photocatalysis material and preparation method thereof, include the following steps: first to mix carbon nanotube with graphene oxide solution, ultrasonic disperse, obtains carbon nanotube/graphene oxide suspension;Acetic acid dihydrate zinc solution is added into carbon nanotube/graphene oxide suspension of acquisition again, ultrasonic disperse obtains mixed solution;Spray drying treatment is carried out to the mixed solution of acquisition, obtains powdered product;Powdered product is placed under inert atmosphere, calcine by steps, it is cooling, obtain graphene micro-flowers/nano zinc oxide photocatalysis material.Catalysis material of the invention has the characteristics that absorption, high activity by force under visible light;Meanwhile the problems such as cumbersome technique faced in nanocatalyst, inefficiency are prepared compared to solwution method, spray drying technology prepares catalysis material, simple, efficient, pollution-free. |