http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108997112-B

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Predicate Object
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-29
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-04
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-29
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-04
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-145
filingDate 2018-07-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-07-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-07-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108997112-B
titleOfInvention Preparation method of 4-acetoxyl-2-methyl-2-butenal
abstract The invention discloses a preparation method of 4-acetoxyl-2-methyl-2-butenal. The method comprises the following steps: (1) under the catalysis of a phase transfer catalyst, chloroisopentene reacts with acetate to generate isopentenol acetate; (2) oxidizing the prenol acetate obtained in the step (1) by using hydrogen peroxide under the catalysis of selenium dioxide to obtain 4-acetoxyl-2-methyl-2-butenal. The method takes the chloroisoamylene as a starting material, is a common fine chemical intermediate, is cheap and easy to obtain, does not need a noble metal catalyst in the reaction process, and has the advantages of low cost, short synthetic route, simple operation and little environmental pollution. Is an effective synthetic route.
priorityDate 2018-07-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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