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filingDate 2018-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108911516-B
titleOfInvention Heterojunction glass ceramic with photocatalytic performance and preparation method thereof
abstract The invention provides heterojunction glass ceramics with photocatalytic performance, which is characterized in that: is Bi 3.64 Mo 0.36 O 6.55 /Bi 2 MoO 6 A heterojunction glass ceramic. The preparation of (1) and the reaction of Bi 2 O 3 And MoO 3 Ball-milling and mixing the mixture according to the molar ratio of 1:1 to obtain uniformly mixed powder, drying the uniformly mixed powder, putting the dried powder into a furnace, heating the dried powder to 650-750 ℃, calcining the powder, cooling the calcined powder along with the furnace to room temperature, and grinding the calcined powder to obtain Bi 2 MoO 6 Crystal powder A; (2) mixing the prepared powder A and Li 2 B 4 O 7 Uniformly mixing the raw materials according to the molar ratio of 3:7, pouring the mixture into a crucible, and heating to 1000-1200 ℃ for calcination; then pouring the melt into water for water quenching, drying and grinding to obtain Bi 3.64 Mo 0.36 O 6.55 Microcrystalline glass powder; (3) bi obtained by the preparation 3.64 Mo 0.36 O 6.55 Pouring the microcrystalline glass powder into the crucible for heat treatment at the temperature of 450-550 ℃, so that crystals in the microcrystalline glass grow up, and the microcrystalline glass with the photocatalytic performance is obtained. Successfully prepares Bi with good photocatalytic performance 3.64 Mo 0.36 O 6.55 /Bi 2 MoO 6 A heterojunction glass ceramic.
priorityDate 2018-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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