http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108904554-A

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filingDate 2018-07-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2018-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108904554-A
titleOfInvention The preparation method of phenols component in a kind of red winter Balaenoptera borealis Lesson
abstract The invention discloses a kind of preparation methods of phenols component in red winter Balaenoptera borealis Lesson, and steps are as follows:Red winter Balaenoptera borealis Lesson herb is crushed, is placed in conical flask, adds petroleum ether, oscillation shakes up, closed and repeatedly shake, 25-35 DEG C of placement 8-10d, filtering volatilize petroleum ether, and addition volume fraction is 85-95% ethyl alcohol, heating and refluxing extraction 2-3h, filtering, filtrate, extracting solution are concentrated under reduced pressure to give medicinal extract;Medicinal extract is separated through silica gel column chromatography, successively uses volume ratio 50:1,30:1,25:1,14:1,5:1 chloroform-methanol elution, collects 14:1 elution fraction, is concentrated to obtain the final product.The preparation method can be effectively obtained phenols component in red winter Balaenoptera borealis Lesson, have anti-asthma, antineoplastic action, furthermore preparation method simple possible, easy to operate, can be mass-produced.
priorityDate 2018-07-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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