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filingDate 2018-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-10-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-10-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108855145-B
titleOfInvention A two-step method for preparing cobalt sulfide/molybdenum sulfide composite material and its application in hydrogen evolution reaction
abstract The invention discloses a two-step method for preparing Co 9 S 8 /MoS 2 composite material and its application in hydrogen evolution reaction. The purpose of the invention is to improve the catalytic performance and self-stability of catalyst for hydrogen evolution reaction. Firstly, a Co 9 S 8 precursor with a hollow sphere structure was obtained by hydrothermal treatment of a mixed solution of cobalt salt, thiourea and glutathione, and then the Co 9 S 8 precursor was placed in molybdenum salt and L-cysteine A second hydrothermal treatment is performed in an acid solution, during which the MoS 2 nanoflower precursor grows on Co 9 S 8 with a hollow sphere structure, and finally Co 9 S 8 /MoS 2 is obtained after calcination. The unique three-dimensional nanostructure of the composite enables it to have a larger specific surface area and expose more active sites; it is worth noting that there is an interface structure between Co 9 S 8 and MoS 2 , and there are Co-Mo-S bonds that help to enhance the catalytic activity, thereby enhancing the catalytic activity for hydrogen evolution. The method is simple to operate, pollution-free in the production process, and easy to produce.
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