http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108821266-B
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2002-85 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2002-80 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2002-01 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2006-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2002-72 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2006-17 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C213-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B32-184 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J27-24 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C213-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J27-24 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C215-76 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B32-184 |
filingDate | 2018-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-01-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-01-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-108821266-B |
titleOfInvention | Preparation method of nitrogen-doped graphene |
abstract | Adding metered lime nitrogen, a carbon source and deionized water into a beaker respectively, controlling the temperature of a water bath at 60-80 ℃, stirring, adjusting the pH of a reaction material to 9-12, reacting for 3-5 h, uniformly spreading the reaction material into an enamel tray, drying, and uniformly grinding the material to obtain solid powder; transferring the solid powder into a porcelain boat, putting the porcelain boat into a tubular furnace for pyrolysis, introducing nitrogen into the furnace for protection, heating the tubular furnace to 540-580 ℃ at a speed of 1-3 ℃/min, preserving heat for 2-3 h, heating to 750-950 ℃ at a speed of 3-8 ℃/min, preserving heat for 1-2 h, then naturally cooling to room temperature, soaking the product with dilute hydrochloric acid, washing with water for multiple times until the product is neutral, and drying to obtain the nitrogen-doped graphene. The method uses cheap lime nitrogen as a raw material, and does not need to use a metal catalyst in the preparation process, thereby reducing the production cost and simplifying the production process. |
priorityDate | 2018-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 60.