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publicationDate 2018-10-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108689798-A
titleOfInvention A method for improving the quality of organosilicon monomer synthesis and recovery of methyl chloride
abstract The invention relates to a method for improving the quality of organic silicon monomer synthesis and recovery of methyl chloride. After the synthetic gas output from the fluidized bed reactor is washed and dedusted by a washing tower and condensed, the condensate is pumped to the methyl chloride tower as a liquid phase. The uncondensed gas is compressed by a compressor and then enters the methyl chloride tower as the gas phase feed; the top of the methyl chloride tower is equipped with two-stage condensers, and the condensate of the first-stage condenser enters the middle tank of methyl chloride as the recovery of methyl chloride, and the second stage The condensate from the condenser enters the reflux tank of the methyl chloride column and is used as the reflux liquid of the column. The present invention changes the recovery of methyl chloride from the traditional side line extraction to the top extraction, and adopts the process method of graded condensation, and at the same time adjusts the gas phase feed of the methyl chloride tower to the top of the liquid phase feed to further improve the quality of the recovered methyl chloride, Ensure the stability of the organic silicon monomer synthesis process.
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