http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108676176-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_bfe41e00679777c040d295aad8366014 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/A61P35-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08H8-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/A61P31-12 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P31-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08H7-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P35-00 |
filingDate | 2018-07-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-10-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-108676176-A |
titleOfInvention | A kind of preparation method of kadsura longepedunculata lignin ingredient |
abstract | The invention discloses a kind of preparation methods of kadsura longepedunculata lignin ingredient, and steps are as follows:Kadsura longepedunculata is extracted 13 times with 65 75% ethyl alcohol cold soaking of volume fraction, 3 5d, merges extracting solution every time, and extracting solution is concentrated under reduced pressure to give medicinal extract;Gained medicinal extract is diluted with water, uses petroleum ether, ethyl acetate and water saturated extracting n-butyl alcohol successively, is concentrated under reduced pressure, obtains acetic acid ethyl ester extract;By acetic acid ethyl ester extract large pore resin absorption column chromatographic isolation, first 7 column volumes are rinsed with 10% ethyl alcohol and remove big polar components, then use 75% ethanol elution, 10 column volumes, 75% eluent is collected, then detach through silica gel column chromatography, successively with volume ratio 46:1、23:1、17:1、5:1 chloroform methanol elution, collects 17:1 elution fraction, concentrates to obtain the final product.Preparation method is simple for this, and obtained lignin ingredient has significant antitumor, antiviral activity, can be used for drug preparation. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113912619-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-115707482-A |
priorityDate | 2018-07-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.