http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108623503-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C315-00 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C315-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C317-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C317-18 |
filingDate | 2018-05-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-01-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-01-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-108623503-B |
titleOfInvention | Green preparation method of vinyl sulfone derivative in water phase |
abstract | The invention relates to a green of a vinyl sulfone derivative in an aqueous phaseA color synthesis method. Adding an olefin compound (1a), a sulfonyl hydrazine compound shown as a formula 2a, tetrabutylammonium iodide (TBAI), tert-butyl alcohol peroxide (TBHP) and solvent water into a Schlenk reaction bottle, placing the reaction bottle at a certain temperature under the condition of air atmosphere, stirring for reaction, monitoring the reaction process by TLC or GC until the raw materials are completely reacted, and carrying out aftertreatment to obtain a target product, namely a vinyl sulfone derivative (I); |
priorityDate | 2018-05-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 72.