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filingDate 2018-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e849e6348964a962be59244122d2aae0
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publicationDate 2018-09-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108586200-A
titleOfInvention A kind of synthesis technology of semisynthetic perfume
abstract The invention discloses a kind of synthesis technologies of semisynthetic perfume, provide synthesis material, including:Lemon eucalyptus oil, containing citronellal 75% 78% in the lemon eucalyptus oil;Raney nickel, the Raney nickel are made up of nickel alumin(i)um alloy;Lemon eucalyptus oil 100g 500g, Raney nickel 2g 5g, 10% potassium hydroxide 1g 2g, triethylamine 1g 3g, methanol 40g 70g and co-catalyst 30g 60g are provided, sucked in the autoclave of 15L successively;Hydrogen is arranged into the autoclave, the hydrogen content in the hydrogen is more than 99%, and for the pressure of the hydrogen for 110Mpa 130Mpa between, hydrogen row 3 times or more is passed through the hydrogen of 5 Mpa of 2Mpa into the autoclave again;The autoclave is heated to 75 degrees Celsius or more, lemon eucalyptus oil is made to generate hydro-reduction reaction;It is continually fed into the hydrogen of 5 Mpa of 2Mpa, until when not inhaling hydrogen, citronellol and the also composition containing tetrahydrogeraniol and dihydrogeraniol are obtained, continual stirring is carried out, and extrudes from the autoclave citronellol and the also composition containing tetrahydrogeraniol and dihydrogeraniol.
priorityDate 2018-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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