http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108558920-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_4baf61b82705468dd1ff913b8ce785f7 |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07B2200-13 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F5-003 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G83-008 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F5-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G83-00 |
filingDate | 2018-04-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a9bc19d392b919283c7a1d32e533e350 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_eec4c18741c5aa2d17ea92d8299881ea http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a939e06a8c21046ee5c94bb0b36d78a7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ec268ffc64c3b967bd6403b967b1150f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_89f3a5d3b7de4a4c0876e0eea4373bd6 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_be9eb0bce66cf8cc1a50357232f848e5 |
publicationDate | 2018-09-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-108558920-A |
titleOfInvention | 4 '-phenyl -2,2 ':The preparation method of 6 ', 2 ' '-terpyridyl nitric acid Gd coordination compound |
abstract | The invention discloses a kind of 4' phenyl 2,2 ':The preparation method of 6 ', 2 ' ' terpyridyl nitric acid Gd coordination compound.Weigh 4' phenyl 2,2 ':6 ', 2 ' ' terpyridyl is dissolved in obtained solution in dichloromethane, and solution is moved into reaction kettle;It weighs gadolinium nitrate hexahydrate and is dissolved in acetonitrile obtained gadolinium nitrate hexahydrate solution, gadolinium nitrate hexahydrate solution is added in reaction kettle, then reaction kettle is placed in electric drying oven with forced convection, isothermal reaction 48 hours at 80 DEG C, it is finally cooled to room temperature, obtain faint yellow acicular crystal, as 4' phenyl 2,2 ':6 ', 2 ' ' terpyridyl nitric acid Gd coordination compound;The complex belongs to rhombic system, and space group is Pbca .The present invention has many advantages, such as simple for process, of low cost, reproducible, has successfully synthesized Gd coordination compound, certain foundation is provided for the complex of synthesizing rare-earth metal. |
priorityDate | 2018-04-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 33.