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filingDate 2018-03-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2018-08-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108396407-A
titleOfInvention A kind of preparation method of AZO hollow Nano fiber in use
abstract The invention discloses a kind of preparation methods of AZO hollow Nano fiber in use, and steps are as follows:PVA particles are dissolved in the mixed liquor being made of glacial acetic acid and deionized water, PVA spinning solutions are stirred to obtain;PVA spinning solutions are placed on electrostatic spinning machine and carry out electrostatic spinning, the tunica fibrosa that metal roller is collected is put into baking oven and is heat-treated;Tunica fibrosa after heat treatment is added in three-necked flask, stirring at low speed in 60 64 DEG C of thermostat water bath is placed on after being infiltrated with deionized water;By Al (NO 3 ) 3 ·9H 2 O and Zn (NO 3 ) 2 ·6H 2 O is dissolved in deionized water, is instilled NaOH solution and zinc salt aluminum salt solution simultaneously to three-necked flask, is continued to stir 2.5 3.5h after titration;After, it takes out tunica fibrosa, is laid on polyfluortetraethylene plate, is dried after cleaning, calcine, cooling to obtain the final product.AZO hollow Nano fiber in use prepared by this method has good photocatalytic degradation of dye performance.
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