http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108383737-A

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filingDate 2018-04-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_76b80a3d11e6e5bf81a493d306988d54
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_af08d4469f07b97722f51f879a88bc05
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publicationDate 2018-08-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108383737-A
titleOfInvention To the solvent-free hydrogenation reduction process of amino trifluomethoxybenzene
abstract The present invention relates to a kind of to the solvent-free hydrogenation reduction process of amino trifluomethoxybenzene, belongs to pesticide chemical product preparation method field;It mainly includes the following steps that:P-nitro-trifluoromethyl is added in reduction reaction kettle in raw material, solvent-free, Raney Ni is under catalysts conditions, carry out hydrogenation reduction, after reaction, catalyst is recovered by filtration under cooling, normal pressure, filtrate negative pressure rectifying can be obtained to amino trifluomethoxybenzene;Whole process of the present invention is all made of solvent-free process condition, reduces the discharge of the organic matter of Conventional process;It overcomes methanol equal solvent and reacts generation carbaryl class by-product with the amino of reduction, improve product purity;More relatively low than existing solvent method temperature, energy consumption is smaller, reduces production cost, is conducive to energy-saving and emission-reduction.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112159329-A
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109134277-A
priorityDate 2018-04-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 35.