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filingDate 2016-11-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bcd5d607ee86d2f3ac82d48b57ae37fa
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publicationDate 2018-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108349806-A
titleOfInvention Synthesis of High Solid Polycarboxylates for Cement Superplasticizers
abstract The present invention provides an efficient method of forming high solids polymeric polyacids or comb polymers useful as superplasticizers or dispersants comprising: at (i) 0.01 to 1 wt. In the presence of a water-soluble free radical initiator or redox couple and (ii) 2 to 22% by weight of one or more phosphorus oxide-containing compounds, the wet reaction mixture is heated to 80 to 100° C. for a first period of time, and then sequentially heated to a second temperature of 150 to 250° C. for a second period of time, the wet reaction mixture having a solids content of 80 to 99% by weight and comprising 15 to 60% by weight of one or more ethylenically unsaturated Acid or salt thereof, 37 to 76.99% by weight of one or more polyether polyols, alkyl polyether polyols, polyetheramines or alkyl polyethers, all weights are based on the total weight of the wet reaction mixture .
priorityDate 2015-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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