http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108329233-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_85a7dbbfe7f01a0f6454543b93101151
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C247-04
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C247-04
filingDate 2018-04-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2d1a55d1a0de576dbcf36d809bf2f98c
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publicationDate 2018-07-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108329233-A
titleOfInvention A kind of preparation method of 1,3- diazidos -2- propyl alcohol
abstract The present invention discloses a kind of preparation method of 2 propyl alcohol of 1,3 diazido, is to solve the problems, such as prior art solvent not environmentally.1,3 dichloro, 2 propyl alcohol is added in deionized water, under stirring, sodium azide is added, is warming up to 80 DEG C~95 DEG C, reacts 5h~8h, wherein the mass ratio of 1,3 dichloro, 2 propyl alcohol, sodium azide and deionized water is 1.0:1.2~1.9:6.0~10.0.After the completion of reaction, dichloromethane extraction, then be washed with deionized three times, vacuum distillation removes dichloromethane, obtains 1,3 diazido of weak yellow liquid, 2 propyl alcohol.The present invention is used for the preparation of 1,3 diazido, 2 propanol compounds.
priorityDate 2018-04-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 28.