http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108321388-B

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filingDate 2018-01-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108321388-B
titleOfInvention Synthesis method of nickel-doped iron disulfide nanowire array structure on titanium sheet substrate
abstract The invention relates to a method for synthesizing a nickel-doped iron disulfide nanowire array structure on a titanium sheet substrate, which comprises the steps of preparing a mixed aqueous solution containing ferric salt, nickel salt, sodium sulfate and urea, putting a clean titanium sheet into the mixed aqueous solution, and carrying out hydrothermal reaction on the titanium sheet to obtain a nickel-doped iron oxide hydroxide nanowire array growing on the surface of the titanium sheet substrate in situ; and (3) placing the precursor in a tubular furnace for high-temperature gas-phase vulcanization, and performing atmosphere protection by using argon to obtain the nickel-doped iron disulfide nanowire array assembled on the titanium sheet substrate. The method is simple and convenient to operate and good in repeatability, the obtained product is stable in structure, can be uniformly and firmly distributed on the surface of the titanium sheet, can be directly used as a two-dimensional electrode material to be applied to electrochemical equipment, and meanwhile, through electrolytic water tests, the doping of nickel greatly improves the electrocatalytic hydrogen production activity and stability of the iron disulfide, is expected to further promote the performance improvement of the iron disulfide in the fields of energy storage, photocatalysis and the like, and expands the application range of the iron disulfide.
priorityDate 2018-01-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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