http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108295872-A

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filingDate 2018-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5a9d0691f368c6c32adba8e9c47a975b
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publicationDate 2018-07-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108295872-A
titleOfInvention A kind of hydro-thermal method preparation Bi2S3/1T@2H-MoS2Method
abstract The present invention discloses hydro-thermal method and prepares Bi 2 S 3 /1T@2H‑MoS 2 As excellent photochemical catalyst and its research of degradable organic pollutant photocatalysis performance under visible light, the preparation method include:1T@2H MoS are prepared first 2 :Using deionized water as solvent, by ammonium heptamolybdate, 30 min of thiocarbamide magnetic agitation, is reacted for 24 hours for 220 DEG C in autoclave, obtain sample H1;H1 is placed in 40ml absolute ethyl alcohols in autoclave after centrifuge washing and reacts 8h for 220 DEG C, 1T@2H MoS are obtained after centrifuge washing drying 2 Nanosphere.Next prepares Bi 2 S 3 /1T@2H‑MoS 2 :By CH 3 CSNH 2 Aqueous solution be added to Bi (NO 3 ) 3 –5H 2 It stirs in the ethanol solution of O and quickly, CO (NH is added thereto later 2 ) 2 Aqueous solution, 30 min of magnetic agitation adds the 1T@2H MoS prepared 2 And stir fully, 120 DEG C are adjusted the temperature in autoclave, keeps 12h, and product centrifuge washing is placed in 60 DEG C of vacuum drying chamber dry 6h, obtains Bi 2 S 3 /1T@2H‑MoS 2 .The present invention uses hydro-thermal method, easy to operate, green safe, of low cost, gained Bi 2 S 3 /1T@2H‑MoS 2 It is excellent to the degradation property of organic dyestuff under visible light.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114887631-B
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114887631-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112121826-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110180560-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110180560-B
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110841661-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109553181-A
priorityDate 2018-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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