http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108285528-A

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filingDate 2018-03-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bb99de5f938af6faac9e4dd90b535c30
publicationDate 2018-07-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108285528-A
titleOfInvention A kind of preparation method of ultrahigh molecular weight medical polylactic acid
abstract The invention discloses a preparation method of ultra-high molecular weight medical polylactic acid. Step 1: Put a certain proportion of lactide monomer, catalyst and initiator into a polymerization reaction container; Step 2: Raise the temperature to make the The mixture undergoes a polymerization reaction to obtain a polymer; step 3: dissolve the obtained polymer with dichloromethane or chloroform, and add a poor solvent to precipitate a crude polylactic acid product; step 4: vacuum-dry the precipitated polylactic acid crude product to obtain The ultra-high molecular weight medical polylactic acid; the catalyst is at least one of stannous octoate, stannous acetate and stannous chloride; the initiator is at least one of dodecanol, 1,4-butanediol and cyclohexane A sort of. The invention does not need segmented reaction, which is beneficial to improve production efficiency and reduce production cost; high-purity lactide is used as raw material to increase the vacuum degree of the reaction system, which is beneficial to the synthesis of ultra-high molecular weight polylactic acid.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114752048-A
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priorityDate 2018-03-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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