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publicationDate 2018-07-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108276247-A
titleOfInvention A kind of anti-form-1, the refining plant of 3- dichloropropylenes
abstract The invention discloses a kind of refining plants of trans- 1,3 dichloropropylene, wherein the tower top feed inlet of rectifying column is connected to head tank by feed pump, and extractant is housed in head tank;The middle part feed inlet of rectifying column is connected to the discharge port of chloropropene device by the trans- 1,3 dichloropropylene pipeline of low concentration;The air inlet of the tower top gas outlet connection condenser of rectifying column, the air inlet of the gas outlet connection deep freezer of condenser, the gas outlet of deep freezer is connected to vacuum pump;The feed inlet of the discharge port connection return tank of condenser, the discharge port of return tank are connected to the overhead reflux mouth of rectifying column by reflux pump, and high concentration trans- 1, the outlet of 3 dichloropropylenes are provided between reflux pump and overhead reflux mouth;The discharge port of deep freezer is connected to impurity recycling can;The bottom of tower of rectifying column is provided with reboiler.The present invention makes trans- 1 by continuous vacuum extraction process, and the concentration of 3 dichloropropylenes reaches 99.5% or more, has been upgraded to the other application of pharmaceutical grade.
priorityDate 2018-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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