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filingDate 2018-02-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-09-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-09-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108250041-B
titleOfInvention Preparation method of fully deuterated methanol
abstract The invention discloses a preparation method of fully deuterated methanol, which comprises the following steps: reacting deuterium gas and carbon monoxide at the reaction pressure of 1-10Mpa and the reaction temperature of 150-550 ℃ in the presence of a catalyst to generate the fully deuterated methanol, wherein the feeding volume ratio of the deuterium gas to the carbon monoxide is 1: 1-10, and the catalyst is one or more of gold oxide, platinum oxide and rhodium oxide; the preparation method of the fully deuterated methanol has the advantages of mild reaction conditions, high reaction yield and simple process operation.
priorityDate 2018-02-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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