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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-12
filingDate 2016-12-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_99d5c5929ff1c172be3822d4caae140d
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_642025c4839ab58a378e7c6e2ec0cbf8
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publicationDate 2018-07-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108238947-A
titleOfInvention A kind of method that no catalyst oxygen oxidation ortho-methylnitrobenzene prepares o-nitrobenzoic acid
abstract A kind of method that no catalyst oxygen oxidation ortho-methylnitrobenzene prepares o-nitrobenzoic acid is related to the preparation method of o-nitrobenzoic acid.Under conditions of any catalyst is not added with, using ortho-methylnitrobenzene as raw material, oxygen is oxidant, sodium hydroxide is alkali, and reaction temperature is 25 85 DEG C, is reacted 5 72 hours in solvent alcohol or its aqueous solution, it is post-treated, it isolates and purifies to obtain the o-nitrobenzoic acid.The method is without catalyst;Raw material and solvent are cheap;And reaction temperature is moderate;Control is readily produced, yield may be up to more than 90%, and prepares and industrialize suitable for a large amount of, have broad application prospects.
priorityDate 2016-12-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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