http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108218810-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D277-78 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D277-78 |
filingDate | 2018-01-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-09-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-09-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-108218810-B |
titleOfInvention | Micro-reaction method for synthesizing 2,2' -dithiodibenzothiazole |
abstract | The invention discloses a method for synthesizing 2,2' -dithiodibenzothiazyl (DM for short) based on a micro mixer. The method uses a micro mixer to rapidly mix a low carbon alcohol solution of 2-mercaptobenzothiazole (M for short) and a low carbon alcohol solution of hydrogen peroxide, then the reaction is finished in a reaction kettle for a certain time, and the production process can be finished after the products are filtered, washed and dried. The method can realize the reaction effects that the conversion rate of M is more than 99%, the yield of DM is more than 98% and the initial melting point is more than 174 ℃, and can efficiently, continuously and safely implement the DM production process. |
priorityDate | 2018-01-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 28.