http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108218386-B

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filingDate 2018-01-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-01-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-01-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108218386-B
titleOfInvention Preparation method of chlorosilane modified graphene oxide/silicon dioxide heat-insulation composite material
abstract The invention belongs to the field of building thermal insulation materials, and discloses a preparation method of a chlorosilane modified graphene oxide/silicon dioxide aerogel composite thermal insulation material, which comprises the following steps: preparing a graphene oxide solution; preparing chlorosilane modified graphene oxide; preparing chlorosilane modified graphene oxide/silicon source sol; preparing modified graphene oxide/silicon dioxide gel; and (3) preparing the modified graphene oxide/silicon dioxide aerogel. According to the invention, the high reaction activity between tetrachlorosilane and hydroxyl is utilized to carry out surface chemical modification on graphene oxide, and the obtained chlorosilane-modified graphene oxide has good dispersibility in an alcohol/water mixed solution of a silicon source precursor. In addition, chlorosilane on the surface of the modified graphene oxide can be used as a reaction active point, so that a strong Si-O-Si chemical bond connection is formed between the modified graphene oxide and a hydrolysate of a silicon source, sufficient cross-linking points between the graphene oxide and a silicon dioxide three-dimensional network are ensured, and an effective mechanical enhancement effect is achieved.
priorityDate 2018-01-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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