http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108033958-B

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D455-04
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D455-03
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D455-03
filingDate 2018-02-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-03-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-03-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108033958-B
titleOfInvention Demethyleneberberinehydrochloride hydrochloride crystal form and preparation method thereof
abstract The invention belongs to field of pharmaceutical chemistry technology, more particularly to four kinds of crystal forms A, B, C, D and preparation method thereof of demethyleneberberinehydrochloride hydrochloride, invention further provides the X-ray ray powder diffraction characteristic absorption peak of this four kinds of crystal forms, infrared absorption peak and DSC map.Crystal form X-ray ray powder diffraction characteristic diffraction peak is about 8.205,8.805,10.817,14.835,15.479,16.668,17.492,18.529,20.656,21.536,23.538,25.657,26.192,28.808 °.The invention further relates to the preparation methods of four kinds of demethyleneberberinehydrochloride hydrochloride crystal forms.It is the preparation method simple process, high income, at low cost;Product purity is high, quality is stablized.
priorityDate 2018-02-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 34.