http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108017542-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-313 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-313 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-716 |
filingDate | 2018-01-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2021-03-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2021-03-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-108017542-B |
titleOfInvention | Pipelining preparation method of oxodicarboxylic acid diethyl ester analogue |
abstract | The invention relates to a canalization preparation method of an oxo-dicarboxylic acid diethyl ester analogue, which comprises the following steps: (1) preparing raw materials: dissolving diethyl dicarboxylate serving as a raw material in butyl acetate for later use; (2) preparing a catalyst: dissolving sodium hypochlorite and acetic acid in water for later use; (3) and (3) oxidation reaction: the raw materials and the catalyst firstly pass through a mixer at a certain flow rate and then enter a pipeline reactor for reaction; (4) and (3) post-treatment: and carrying out reduced pressure distillation to obtain a target product. The invention improves the quality of the product, reduces the reaction time, reduces the cost, has simple and safe operation, ensures clean, environment-friendly and efficient production of the product and is more suitable for mass production. |
priorityDate | 2018-01-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 31.