http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108017542-B

Outgoing Links

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-54
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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-54
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-313
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-716
filingDate 2018-01-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-03-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-03-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-108017542-B
titleOfInvention Pipelining preparation method of oxodicarboxylic acid diethyl ester analogue
abstract The invention relates to a canalization preparation method of an oxo-dicarboxylic acid diethyl ester analogue, which comprises the following steps: (1) preparing raw materials: dissolving diethyl dicarboxylate serving as a raw material in butyl acetate for later use; (2) preparing a catalyst: dissolving sodium hypochlorite and acetic acid in water for later use; (3) and (3) oxidation reaction: the raw materials and the catalyst firstly pass through a mixer at a certain flow rate and then enter a pipeline reactor for reaction; (4) and (3) post-treatment: and carrying out reduced pressure distillation to obtain a target product. The invention improves the quality of the product, reduces the reaction time, reduces the cost, has simple and safe operation, ensures clean, environment-friendly and efficient production of the product and is more suitable for mass production.
priorityDate 2018-01-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 31.