http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107915249-B

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filingDate 2016-10-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-03-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-03-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107915249-B
titleOfInvention Nano Cu of square core-shell structure2O/Cu3Preparation method of N material
abstract The invention relates to nano Cu with a square core-shell structure 2 O/Cu 3 The preparation method of the N material mainly adopts an acid-base micro-etching method, takes copper chloride as copper salt, takes sodium dodecyl benzene sulfonate as a surfactant, and takes sodium hydroxide and hydroxylamine hydrochloride as etching agents, and the two are added in different proportions; heating in water bath at 40-90 deg.c for 10min, and centrifuging to separate the precursor. Generated Cu 2 O is nitrided again, and Cu is then added 2 Nitriding the O material for 1-4 hours at 200-250 ℃. Can obtain the nano Cu with the square core-shell structure 2 O/Cu 3 And (3) N material. The method has the advantages of simple and convenient synthesis method, low reaction temperature and the like.
priorityDate 2016-10-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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