http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107814715-A

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-62
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-48
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-24
filingDate 2016-09-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_360efd7e974f7c9f0b1b64d930a2abb6
publicationDate 2018-03-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107814715-A
titleOfInvention The preparation method of butyl caprylate
abstract The present invention relates to a kind of preparation method of butyl caprylate, this method comprises the following steps:(1) step of esterification, octanoic acid, the concentrated sulfuric acid, is put into reactor butanol, stirring, is heated to boiling reaction, keeps boiling reflux state to separate moisture therein;(2) water-washing step, water will be added in the mixture after esterification, after stirring, stratification, remove water layer therein;(3) dealcoholysis step;(4) purification step, will add refining agent in the crude product after dealcoholysis, stirring is refined one hour;(5) filtration step.The preparation method of this butyl caprylate have it is easy to operate, it is simple and easy to be easy to implement industrialized production, improve production efficiency.
priorityDate 2016-09-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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