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filingDate 2016-09-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107814576-B
titleOfInvention In-situ reaction for preparing MB2Method for preparing (E) -MC-BN ultrahigh temperature ceramic matrix composite material
abstract The invention belongs to the field of ultra-high temperature ceramics, and particularly relates to an in-situ reaction preparation methodSpare MB 2 -MC-BN ultra high temperature ceramic matrix composite material. The raw materials consist of MN powder (M ═ Ti, Zr, Hf or Ta) and B 4 C powder is mixed and then is subjected to in-situ reaction hot-pressing sintering in a hot-pressing furnace or reaction sintering in a discharge plasma sintering furnace. Under the protective atmosphere, the heating rate is 10-100 ℃/min, the sintering temperature is 1900-2100 ℃, the sintering time is 10 min-2 h, the sintering pressure is 20 MPa-40 MPa, and finally the MB is obtained 2 -MC-BN composite materials (M ═ Ti, Zr, Hf or Ta) which are candidates for high temperature resistant structural elements such as the nozzle throat of solid rocket engines or the nose cone, wing leading edge of very high speed aircraft.
priorityDate 2016-09-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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