http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107778400-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_9aea490eb2a4a9a51e7b126e662c2135 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08F136-08 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F4-48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F2-38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F136-08 |
filingDate | 2017-11-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_07aea3c31fd31480f25fa004746a5a90 |
publicationDate | 2018-03-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107778400-A |
titleOfInvention | A kind of synthetic method of high-cis lithium system isoprene rubber |
abstract | The present invention relates to technical field of petrochemical industry, and in particular to a kind of synthetic method of high-cis lithium system isoprene rubber.A kind of synthetic method of high-cis lithium system isoprene rubber, comprises the following steps:The preparation of raw material:Isoprene, n-BuLi, hexamethylene;The synthesis of lithium system isoprene rubber:High purity N is used first 2 Reactor is cleaned 3 times;5ml solvent and 5g isoprene monomers is added into the reactor after cleaning;Start stirred autoclave until well mixed;When temperature reaches initiation temperature, a small amount of n-BuLi imurity-removal is added;A certain amount of n-BuLi initiation reaction is added after removal of impurities, is eventually adding terminator terminating reaction;Above-mentioned glue condenses by vapor, and carries out extrusion dehydration drying.By the isoprene rubber better performances that the synthetic method of high-cis lithium system isoprene rubber provided by the invention is worth, usage time length is pure, to cut yield without gel higher, suitable for promoting the use of a large area. |
priorityDate | 2017-11-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 27.