http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107778400-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_9aea490eb2a4a9a51e7b126e662c2135
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08F136-08
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F4-48
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F2-38
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F136-08
filingDate 2017-11-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_07aea3c31fd31480f25fa004746a5a90
publicationDate 2018-03-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107778400-A
titleOfInvention A kind of synthetic method of high-cis lithium system isoprene rubber
abstract The present invention relates to technical field of petrochemical industry, and in particular to a kind of synthetic method of high-cis lithium system isoprene rubber.A kind of synthetic method of high-cis lithium system isoprene rubber, comprises the following steps:The preparation of raw material:Isoprene, n-BuLi, hexamethylene;The synthesis of lithium system isoprene rubber:High purity N is used first 2 Reactor is cleaned 3 times;5ml solvent and 5g isoprene monomers is added into the reactor after cleaning;Start stirred autoclave until well mixed;When temperature reaches initiation temperature, a small amount of n-BuLi imurity-removal is added;A certain amount of n-BuLi initiation reaction is added after removal of impurities, is eventually adding terminator terminating reaction;Above-mentioned glue condenses by vapor, and carries out extrusion dehydration drying.By the isoprene rubber better performances that the synthetic method of high-cis lithium system isoprene rubber provided by the invention is worth, usage time length is pure, to cut yield without gel higher, suitable for promoting the use of a large area.
priorityDate 2017-11-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 27.