http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107699001-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09B62-51 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09B67-0072 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B62-51 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B67-24 |
filingDate | 2017-09-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2019-07-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2019-07-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107699001-B |
titleOfInvention | A kind of preparation method of active scarlet dye |
abstract | The present invention relates to a kind of preparation method of active scarlet dye, include the following steps: to be added to Cyanuric Chloride in ice water and carry out mashing processing, obtains mashing liquid;Solid para-ester is added in mashing liquid, mixed ammonium/alkali solutions is continuously added and carries out alkali tune, primary condensation reaction is carried out and obtains a contracting object;The mixed base is soda ash and sodium bicarbonate;Solid J acid is added in a contracting object, condensation reaction is carried out, obtains two contracting things;Continue in the two contracting things for being added to solid H acid, carry out condensation reaction, obtains mixing two contracting things;The molar ratio of the solid J acid and solid H acid is 0.65~0.68:0.32~0.35;Hydrochloric acid is added into Sulpho Tobias Acid and sodium nitrite carries out diazo-reaction, obtains Sulpho Tobias Acid diazonium salt;In the mixing two contracting things that Sulpho Tobias Acid diazonium salt is added to, coupling reaction is carried out, post-processing obtains active scarlet dye.The preparation method is convenient, resource occupation is few, low energy consumption and is easy to mix colours. |
priorityDate | 2017-09-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 36.