http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107628646-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09D11-328 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09D7-61 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08K3-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G49-00 |
filingDate | 2017-10-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2019-08-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2019-08-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107628646-B |
titleOfInvention | A kind of siderochrome mineral black and preparation method thereof |
abstract | The invention discloses a kind of siderochrome mineral black and preparation method thereof, include the following steps: to weigh Cr (NO with Cr:Fe 1~1.85:1 of molar ratio 3 ) 3 ·9H 2 O and Fe (NO 3 ) 3 ·9H 2 O is simultaneously added in the water that heating temperature is 50~70 DEG C, stirs and Cr/Fe aqueous solution is made;The incendiary agent reacted completely therewith is added, and continues heating stirring until all dissolutions;Mixed liquor heating evaporation is concentrated, then solution is placed in the Muffle furnace of 250~300 DEG C of heat preservations and causes self-propagating combustion;Combustion product is placed in high-temperature calcination stove, is risen to 850~1050 DEG C with 5~10 DEG C/min heating rate and is kept the temperature 1~3h, it is siderochrome mineral black that calcined powder is collected in cooling.The present invention is resulting between 0.1~1.0 μm of pigment particle distribution, the mellow and full rule of shape, and crystallinity is high.Product TSR >=31% is higher than similar products at home and abroad. |
priorityDate | 2017-10-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 48.