http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107556431-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F2-38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/D01F9-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F220-48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/D01F6-38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F220-56 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F2-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F222-02 |
filingDate | 2017-09-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-11-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-11-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107556431-B |
titleOfInvention | A kind of method that dimethyl sulfoxide method continuous polymerization prepares polyacrylonitrile solution |
abstract | This application discloses the polyacrylonitrile solutions that a kind of method of dimethyl sulfoxide method continuous polymerization preparation polyacrylonitrile solution and this method obtain.The method for wherein preparing polyacrylonitrile solution includes the following steps:(1) the first-third comonomer and dimethyl sulfoxide (DMSO) are configured to mixed liquor by a certain percentage;(2) mixed liquor is continuously pumped into polymeric kettle, while the dimethyl sulphoxide solution containing initiator is added drop-wise in polymeric kettle;(3) control temperature of reaction kettle is stepped up to 50~70 DEG C from 25 DEG C, when comonomer conversions are 60~63%, polymer fluid is discharged to terminate reaction;(4) polymer fluid is transferred to de- single device and carries out de- single deaeration processing to get finished product.The application is put forward for the first time synthesizes polyacrylonitrile solution with middle conversion ratio, prevents macromolecule from crosslinking generation gel;The polyacrylonitrile solution molecular weight distributing index D that the application obtains is 1.2~2.0, and isotaxy content is 30~34.5%. |
priorityDate | 2017-09-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 31.