http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107556180-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C46-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C50-08 |
filingDate | 2017-09-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2021-03-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2021-03-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107556180-B |
titleOfInvention | Method for preparing and synthesizing 3,3',5,5' -tetramethyl-4, 4' -biphenyl diquinone by ultrasonic rapid method |
abstract | The invention discloses a method for preparing and synthesizing 3,3',5,5' -tetramethyl-4, 4 '-biphenyl diquinone by an ultrasonic rapid method, which adopts 2, 6-dimethylphenol as a raw material for the first time, adds a copper-amine complex catalyst under the condition that alcohol and water are used as solvents, and dropwise adds hydrogen peroxide as an oxidant at a certain speed within a certain time, controls the reaction temperature and the pH value to carry out ultrasonic reaction, and can rapidly obtain an oxidative coupling product 3,3',5,5 '-tetramethyl-4, 4' -biphenyl diquinone after the reaction for a period of time. |
priorityDate | 2017-09-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 49.