http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107540600-B

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Predicate Object
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D211-60
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B57-00
filingDate 2016-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2019-07-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2019-07-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-107540600-B
titleOfInvention A kind of recoverying and utilizing method of AVM hereinafter Batan intermediate production waste liquid
abstract The present invention relates to a kind of recoverying and utilizing methods of AVM hereinafter Batan intermediate production waste liquid, using generated waste liquid in AVM hereinafter Batan intermediate 5R- benzyloxy amino piperidine -2S- formic acid ester oxalate IIb production process as starting material, 5- benzyloxy imino piperidines -2S- formic acid esters III is generated through peroxidating, the chosen property reduction of III, chiral crystallization split, solid 5R- benzyloxy amino piperidine -2S- formic acid ester oxalate IIb are obtained by filtration, and gained filtrate repeats the above oxidation, reduction, split process.The neutralized preparation 5R- benzyloxy amino piperidine -2S- formic acid esters IIa of compound IIb, can prepare AVM hereinafter Batan I using gained compound IIa or compound IIb.Operation of the present invention is easy, improves atom utilization, the final total recovery of compound IIb advantageously reduces cost up to 99.0% or more, advantageously reduces the waste liquid of AVM hereinafter Batan, be conducive to environmental protection.
priorityDate 2016-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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