http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-107512729-B
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2006-80 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01P2002-72 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B39-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C2-86 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C2-66 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J29-40 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J29-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C15-073 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B39-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C2-66 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C2-86 |
filingDate | 2016-06-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-04-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-04-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-107512729-B |
titleOfInvention | Preparation method of binder-free ZSM-5 molecular sieve |
abstract | The invention relates to a preparation method of a binderless ZSM-5 molecular sieve, which mainly solves the problems of long secondary crystallization time, incomplete crystallization and poor catalytic performance in the preparation process of the binderless ZSM-5 molecular sieve in the prior art. The invention adopts the following steps: a) providing a synthetic ZSM-5 molecular sieve; b) mixing the synthesized ZSM-5 molecular sieve with a binder, a pore-forming agent and an aqueous solution of acid, forming and drying to obtain a ZSM-5 molecular sieve precursor; the binder is selected from at least one of silica sol or alumina; wherein the silica sol provides a first silicon source, and the alumina provides a first aluminum source; c) crystallizing a mixture of the ZSM-5 molecular sieve precursor, a second silicon source, a second aluminum source, an alkali source, an organic template and water, and separating and drying a solid product to obtain the binderless ZSM-5 molecular sieve; controlling the total Si/Al molar ratio SiO in the first Si source, the second Si source, the first Al source and the second Al source 2 /Al 2 O 3 The technical scheme of 25-100 better solves the problem and can be used for industrial production of the binder-free ZSM-5 molecular sieve. |
priorityDate | 2016-06-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 90.